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【英文标准名称】:StandardGuideforEstablishingCalibrationforaMeasurementMethodUsedtoAnalyzeNuclearFuelCycleMaterials
【原文标准名称】:用于分析核燃料循环材料的测量方法用校准方法的确定的标准指南
【标准号】:ASTMC1156-2003
【标准状态】:现行
【国别】:
【发布日期】:2003
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:C26.08
【标准类型】:(Guide)
【标准水平】:()
【中文主题词】:说明书;分析;测量方法;校正;燃料循环
【英文主题词】:calibration;calibrationprocedure;calibrationstandard;certifiedreferencematerial(CRM);laboratoryequipment
【摘要】:Calibrationisafundamentalpartofmakingmeasurementsanditseffectonthequalityofmeasurementdataissignificant.Thus,sufficientattentionmustbegiventocalibrationwhenitisestablishedforameasurementmethodsothatthedataproducedwillbeacceptable.Theuseofaninappropriatecalibrationstandard,inadequateinstructionsforcalibration,andpoordocumentationofthecalibrationprocessareexamplesofcircumstancesthatcanadverselyaffectthevalidityofacalibration.Thus,thecalibrationprocessmustconformtocriteriaestablishedtoensurethevalidityofcalibrationresults.SuchcriteriaaregiveninGuideC1009,inwhichcalibrationisidentifiedasacomponentoflaboratoryqualityassurance(seeFig.1).Thisguideexpandsuponthosecriteriatoprovidemorecomprehensiveguidanceforestablishingcalibration.Themannerofcalibrationandothertechnicalrequirementsforcalibratingameasurementmethodareusuallyestablishedwhenamethodisfirstintroducedintoalaboratory,whichmaybethroughvalidationandqualificationasdefinedbyGuideC1068(seeFig.1).However,calibrationinvolvesmorethanthetechnicalaspectsofthecalibrationprocess.Theotherdimensionoftheprocessistheoperationalrequirementsthatarenecessarytoensurethatcalibrationresultsarevalidandthattheyaredocumentedandverifiableshouldtheirintegritybequestioned.Theprovisionsofthisguideprovidethoseoperationalrequirementsandshouldbeconsideredwhenevercalibrationisplannedandestablished.FIG.1QualityAssuranceofAnalyticalLaboratoryData1.1Thisguideprovidesthebasisforestablishingcalibrationforameasurementmethodtypicallyusedinananalyticalchemistrylaboratoryanalyzingnuclearmaterials.Guidanceisincludedforsuchactivitiesaspreparingacalibrationprocedure,selectingacalibrationstandard,controllingcalibratedequipment,anddocumentingcalibration.Theguideisgenericandanyrequiredtechnicalinformationspecificforagivenmethodmustbeobtainedfromothersources.1.2Theguidanceinformationisprovidedinthefollowingsections:SectionGeneralConsiderations4CalibrationProcedure5CalibrationStandard6ControlofCalibratedEquipment7Documentation8Keywords9